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How to make TCPO (for making glow sticks)

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How to make TCPO or bis(2,4,6-trichlorophenyl) oxalate, used in glow stick reactions. WARNING: This procedure should only be performed by, or under the direct supervision of, an experienced chemist. Please refer to the material safety data sheets of all chemicals for their hazards. Synthesis must be performed in a fumehood. Full written procedure can be found at our website:

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